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Photothermal speckle modulation for noncontact materials characterization

Summary

We have developed a noncontact, photothermal materials characterization method based on visible-light speckle imaging. This technique is applied to remotely measure the infrared absorption spectra of materials and to discriminate materials based on their thermal conductivities. A wavelength-tunable (7.5-8.7 um), intensity-modulated, quantum cascade pump laser and a continuous-wave 532 nm probe laser illuminate a sample surface such that the two laser spots overlap. Surface absorption of the intensity-modulated pump laser induces a time-varying thermoelastic surface deformation, resulting in a time-varying 532 nm scattering speckle field from the surface. The speckle modulation amplitude, derived from a series of visible camera images, is found to correlate with the amplitude of the surface motion. By tuning the pump laser's wavelength over a molecular absorption feature, the amplitude spectrum of the speckle modulation is found to correlate to the IR absorption spectrum. As an example, we demonstrate this technique for spectroscopic identification of thin polymeric films. Furthermore, by adjusting the rate of modulation of the pump beam and measuring the associated modulation transfer to the visible speckle pattern, information about the thermal time constants of surface and sub-surface features can be revealed. Using this approach, we demonstrate the ability to distinguish between different materials (including metals, semiconductors, and insulators) based on differences in their thermal conductivities.
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Summary

We have developed a noncontact, photothermal materials characterization method based on visible-light speckle imaging. This technique is applied to remotely measure the infrared absorption spectra of materials and to discriminate materials based on their thermal conductivities. A wavelength-tunable (7.5-8.7 um), intensity-modulated, quantum cascade pump laser and a continuous-wave 532 nm...

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Evaluation of the baseline NEXRAD icing hazard project

Published in:
37th Conference on Radar Meteorology, 14-18 September 2015

Summary

MIT Lincoln Laboratory has developed an icing hazard product that is now operational throughout the NEXRAD network. This initial version of the Icing Hazard Levels (IHL) algorithm is predicated on the presence of graupel as determined by the NEXRAD Hydrometeor Classification Algorithm (HCA). Graupel indicates that rime accretion on ice crystal aggregates is present. It is inferred that the riming process occurs at the altitude that HCA reports graupel as well as to some vertical depth above. To capture some of that depth, temperature and relative humidity interest fields are computed from meteorological model data based on the technique used in the National Center for Atmospheric Research's Current Icing Potential Product and utilized within IHL as warranted. A critical aspect of the IHL development has focused on the verification of the presence of icing. Two methods are used. For the first, pilot reports of icing (PIREPs) are used to score the performance of IHL. Since PIREPs are provided with inherent time and space uncertainties, a buffer of influence is associated with each PIREP when scoring IHL. Results show the IHL as configured is an effective indicator of a potential icing hazard when HCA graupel classifications are present. Results also show the importance of radar volume coverage pattern selection in detecting weak returns in winter weather. For the second, in situ icing missions were performed within range of a dual pol NEXRAD to provide quantitative data to identify the presence of supercooled liquid water. Comparisons of in situ data to HCA classifications show that HCA graupel indications do not fully expose the icing hazard and these findings are being used to direct future attention of IHL development. This paper will describe the verification method and performance assessment of the IHL initial capability.
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Summary

MIT Lincoln Laboratory has developed an icing hazard product that is now operational throughout the NEXRAD network. This initial version of the Icing Hazard Levels (IHL) algorithm is predicated on the presence of graupel as determined by the NEXRAD Hydrometeor Classification Algorithm (HCA). Graupel indicates that rime accretion on ice...

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Aircraft in situ validation of hydrometeors and icing conditions inferred by ground-based NEXRAD polarimetric radar

Published in:
SAE Int. Conf. on Icing of Aircraft, Engines, and Structures, ICE 2015, 15 June 2015.

Summary

MIT Lincoln Laboratory is tasked by the U.S. Federal Aviation Administration to investigate the use of the NEXRAD polarimetric radars for the remote sensing of icing conditions hazardous to aircraft. A critical aspect of the investigation concerns validation that has relied upon commercial airline icing pilot reports and a dedicated campaign of in situ flights in winter storms. During the month of February in 2012 and 2013, the Convair-580 aircraft operated by the National Research Council of Canada was used for in situ validation of snowstorm characteristics under simultaneous observation by NEXRAD radars in Cleveland, Ohio and Buffalo, New York. The most anisotropic and easily distinguished winter targets to dual pol radar are ice crystals. Accordingly, laboratory diffusion chamber measurements in a tightly-controlled parameter space of temperature and humidity provide the linkage between shape and the expectation for the presence/absence of water saturation conditions necessary for icing hazard in situ. In agreement with the laboratory measurements pertaining to dendritic and hexagonal flat plate crystals, the aircraft measurements have verified the presence of supercooled water in mainly low concentrations coincident with regions showing layered anomalies of positive differential reflectivity (ZDR) by ground-based radar, otherwise known as +ZDR 'bright bands'. Extreme values of ZDR (up to +8 dB) have also been found to be coincident with hexagonal flat plate crystals and intermittent supercooled water, also consistent with laboratory measurements. The icing conditions found with the anisotropic description are considered non-classical (condensation/collision-coalescence) and require the ascent of air and availability of ice nuclei. A modest ascent rate (
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Summary

MIT Lincoln Laboratory is tasked by the U.S. Federal Aviation Administration to investigate the use of the NEXRAD polarimetric radars for the remote sensing of icing conditions hazardous to aircraft. A critical aspect of the investigation concerns validation that has relied upon commercial airline icing pilot reports and a dedicated...

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Measurements of differential reflectivity in snowstorms and warm season stratiform systems

Summary

The organized behavior of differential radar reflectivity (ZDR) is documented in the cold regions of a wide variety of stratiform precipitation types occurring in both winter and summer. The radar targets and attendant cloud microphysical conditions are interpreted within the context of measurements of ice crystal types in laboratory diffusion chambers in which humidity and temperature are both stringently controlled. The overriding operational interest here is in the identification of regions prone to icing hazards with long horizontal paths. Two predominant regimes are identified: category A, which is typified by moderate reflectivity (from 10 to 30 dBZ) and modest +ZDR values (from 0 to 13 dB) in which both supercooled water and dendritic ice crystals (and oriented aggregates of ice crystals) are present at a mean temperature of -13 degrees C, and category B, which is typified by small reflectivity (from -10 to +10 dBZ) and the largest +ZDR values (from +3 to +7 dB), in which supercooled water is dilute or absent and both flat-plate and dendritic crystals are likely. The predominant positive values for ZDR in many case studies suggest that the role of an electric field on ice particle orientation is small in comparison with gravity. The absence of robust +ZDR signatures in the trailing stratiform regions of vigorous summer squall lines may be due both to the infusion of noncrystalline ice particles (i.e., graupel and rimed aggregates) from the leading deep convection and to the effects of the stronger electric fields expected in these situations. These polarimetric measurements and their interpretations underscore the need for the accurate calibration of ZDR.
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Summary

The organized behavior of differential radar reflectivity (ZDR) is documented in the cold regions of a wide variety of stratiform precipitation types occurring in both winter and summer. The radar targets and attendant cloud microphysical conditions are interpreted within the context of measurements of ice crystal types in laboratory diffusion...

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Validation of NEXRAD radar differential reflectivity in snowstorms with airborne microphysical measurements: evidence for hexagonal flat plate crystals

Summary

This study is concerned with the use of cloud microphysical aircraft measurements (the Convair 580) to verify the origin of differential reflectivity (ZDR) measured with a ground-based radar (the WSR-88D KBUF radar in Buffalo, New York). The underlying goal is to make use of the radar measurements to infer the presence or absence of supercooled water, which may pose an icing hazard to aircraft. The context of these measurements is the investment by the Federal Aviation Administration in the use of NEXRAD polarimetric radar and is addressed in the companion paper by Smalley et al. (2013, this Conference). The highlight of the measurements on February 28, 2013 was the finding of sustained populations of hexagonal flat plate crystals over a large area northwest of the KBUF radar, in conditions of dilute and intermittent supercooled water concentration. Some background discussion is in order prior to the discussion of the aircraft/radar observations that form the main body of this study. The anisotropy of hydrometeors, the role of humidity and temperature in crystal shape, and the common presence of hexagonal flat plate crystals in the laboratory cold box experiment are all discussed in turn.
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Summary

This study is concerned with the use of cloud microphysical aircraft measurements (the Convair 580) to verify the origin of differential reflectivity (ZDR) measured with a ground-based radar (the WSR-88D KBUF radar in Buffalo, New York). The underlying goal is to make use of the radar measurements to infer the...

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Retroreflectors for remote readout of colorimetric sensors

Published in:
Sensors and Actuators B-Chemical, Vol. 160, No. 1, 15 December 2011, pp. 1244-1249.

Summary

We have developed a remote detection system consisting of commercially available retroreflective material coated with an analyte-specific colorimetric dye. Quantitative performance modeling predicts that, given the appropriate indicator dye, a system with a 10 cm optic and eye-safe illumination should be capable of detecting small droplets of contamination at kilometer ranges. We have synthesized new colorimetric dyes specific to organophosphate contamination and, with these dyes, demonstrated detection of 1um of liquid malathion at over 150 m with less than 20 mW of laser illumination.
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Summary

We have developed a remote detection system consisting of commercially available retroreflective material coated with an analyte-specific colorimetric dye. Quantitative performance modeling predicts that, given the appropriate indicator dye, a system with a 10 cm optic and eye-safe illumination should be capable of detecting small droplets of contamination at kilometer...

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Noncontact optical detection of explosive particles via photodissociation followed by laser-induced fluorescence

Published in:
Opt. Express, Vol. 19, No. 19, 12 September 2011, pp. 18671-18677.

Summary

High-sensitivity (ng/cm2) optical detection of the explosive 2,4,6- trinitrotoluene (TNT) is demonstrated using photodissociation followed by laser-induced fluorescence (PD-LIF). Detection occurs rapidly, within 6 laser pulses (~7 ns each) at a range of 15 cm. Dropcasting is used to create calibrated samples covering a wide range of TNT concentrations; and a correspondence between fractional area covered by TNT and PD-LIF signal strength is observed. Dropcast data are compared to that of an actual fingerprint. These results demonstrate that PD-LIF could be a viable means of rapidly and remotely scanning surfaces for trace explosive residues.
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Summary

High-sensitivity (ng/cm2) optical detection of the explosive 2,4,6- trinitrotoluene (TNT) is demonstrated using photodissociation followed by laser-induced fluorescence (PD-LIF). Detection occurs rapidly, within 6 laser pulses (~7 ns each) at a range of 15 cm. Dropcasting is used to create calibrated samples covering a wide range of TNT concentrations; and...

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Development of dual polarization aviation weather products for the FAA

Published in:
34th Conf. on Radar Meteorology, 5-9 October 2009.

Summary

Weather radar products from the United States' NEXRAD network are used as key components in FAA weather systems such as CIWS, ITWS, and WARP. The key products, High Resolution VIL (HRVIL) and High Resolution Enhanced Echo Tops (HREET), provide primary information about precipitation location and intensity. The NEXRAD network will become dual polarization capable beginning in late 2010 adding the ability to classify hydrometeors. This new aspect from radar remote sensing of the weather offers opportunity to provide new aviation weather products and augment existing ones. This paper will detail the dual polarization product development program at MIT Lincoln Laboratory (LL) in support of FAA system needs. Current development efforts focus on four products. Two new products will provide volumetric analysis seeking aviation hazards (icing and hail). Two existing products, HRVIL and HREET, will be invigorated by dual polarization data to yield improved data quality and mitigation of partial beam blockage. The LL program has partnered with NCAR and NSSL subject matter experts to bring their most advanced research results into these new and improved products. The LL program also has partnered with Valparaiso University for them to provide dual polarization and local sonde sounding data especially during suspected icing conditions. The new Icing Hazards Level (IHL) product is expected to provide the most benefit to the FAA. Its development also poses the greatest challenge both in scope and in the ability of S-band radar to sense the phenomena of interest. Icing phenomena include supercooled drops/droplets and ice crystals and the associated aviation hazard could be aloft or near/at the surface. Graupel is an indication that supercooled water has accreted to ice particles. The initial NEXRAD hydrometeor classifier will not have an explicit supercooled water class or the benefit of supporting data. It will have ice crystal and graupel classes. The LL approach will utilize at least some additional data (vertical thermodynamic profiles). Techniques applied to the development of IHL will likely have applicability to the other products as well. Aspects of the IHL development will also be discussed in the paper.
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Summary

Weather radar products from the United States' NEXRAD network are used as key components in FAA weather systems such as CIWS, ITWS, and WARP. The key products, High Resolution VIL (HRVIL) and High Resolution Enhanced Echo Tops (HREET), provide primary information about precipitation location and intensity. The NEXRAD network will...

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A novel method for remotely detecting trace explosives

Published in:
Lincoln Laboratory Journal, Vol. 17, No. 2, December 2008, pp. 27-40.

Summary

The development of a technique with the ability to detect trace quantities of explosives at a distance is of critical importance. In numerous situations when explosive devices are prepared, transported, or otherwise handled, quantifiable amounts of the explosive material end up on surfaces. Rapid detection of these chemical residues in a noninvasive standoff manner would serve as an indicator for attempts at concealed assembly or transport of explosive materials and devices. We are investigating the use of a fluorescence-based technique to achieve the necessary detection sensitivity.
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Summary

The development of a technique with the ability to detect trace quantities of explosives at a distance is of critical importance. In numerous situations when explosive devices are prepared, transported, or otherwise handled, quantifiable amounts of the explosive material end up on surfaces. Rapid detection of these chemical residues in...

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Proton irradiations of large area Hg(1-x)Cd(x)Te photovoltaic detectors for the cross-track infrared sounder

Published in:
SPIE Vol. 4820, Pt. 1, Infrared Technology and Applications XXVIII, 7-11 July 2002, pp. 479-490.

Summary

The effect of radiation on Hg(1-x)Cd(x)Te photodiodes is an important parameter to understand when determining the long-term performance limitations for the Cross-track Infrared Sounder (CrIS), a Fourier Transform interferometric sensor that will fly as part of the National Polar-orbiting Operational Enviornmental Satellite System (NPOESS). The CrIS sensor uses relatively large area photovoltaic detectors, 1mm in diameter. Each p-on-n Hg(1-x)Cd(x)Te photodiode consists of MBE grown, n-type material on lattice matched CdZnTe, with arsenic implantation used to form the junction. A 1mm diameter detector is achieved by using a lateral collection. Solar, and trapped protons are a significant source of radiation in the NPOESS 833 km orbits. We irradiated 22 LWIR detectors with protons at the Harvard Cyclotron Laboratory (HCL) and monitored the I-V performance and dynamic impedance of each detector. Three groups of detectors were irradiated with either 44, 99, 153-MeV protons, each between 1x10(10) - 4x10(12) p+/cm(2) (total range ~ 0.7 - 690 krad(Si)). Several I-V data sets were collected within that fluence range at all three energies. All the detectors were warmed to room temperature for approximately 96 hours following the largest proton dose, recooled, and then re-characterized in terms of I-V performance and dynamic impedance. The total noise increase predicted for CrIS after 7-years in orbit is less than 1%.
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Summary

The effect of radiation on Hg(1-x)Cd(x)Te photodiodes is an important parameter to understand when determining the long-term performance limitations for the Cross-track Infrared Sounder (CrIS), a Fourier Transform interferometric sensor that will fly as part of the National Polar-orbiting Operational Enviornmental Satellite System (NPOESS). The CrIS sensor uses relatively large...

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